Laboratory in organic chemistry

elementary

BI1_U09, BI1_K02, K03

level: basic

Goals: To teach students basic techniques used in organic laboratory

To teach students basic techniques used in organic laboratory, every student is going to carry out 5 experiments

1) synthesis of acetanilide

2) nitration of acetanilide

3) synthesis of buthyl acetate

4) synthesis of aspirin

5) synthesis of tetraphenylporphyrin

evaluation method: test + report for every experiment

Compulsory (in Polish): Podręcznik do ćwiczeń "Laboratorium chemiczne", Wydanie II, 2005, Wydawnictwo UKSW

Voluntary: R. T. Morrison, R. N. Boyd “Organic Chemistry” Prentice Hall, 1992.

G. Patrick “Instant Notes in Organic Chemistry" Taylor & Francis, 2003

BI_W02 - has knowledge of organic chemistry, knows assessment methods and criteria,

BI_W06 - knows, understands and follows safety rules at the laboratory.

Skills:

BI_U04 - conducts simple laboratory experiments under the scientific supervision

BI_U06 - conducts simple chemical experiments

Competencies:

BI_K02 - works in a team

BI_K06 - is responsible for his own safety, as well as safety of others working in the laboratory, in case of emergency is able to react properly

Number of ECTS points - 3

Laboratory attendance - 30 hours

Preparation to the exercises - 15 hours

Report preparation -15 hours

Preparation to the final test - 30 hours

Total number of hours - 90

ECTS: 90 hr./30hr. = 3

Final score is based on the results of:

1) entry tests concerning the exercises (rules and working methods),

2) written reports describing each exercise (containing problem description, obtained results and calculations)

-3) final test concerning all exercises and used laboratory technics

Knowledge (BI_W03, BI_W09)

score 2 (not satisfactory): student doesn’t have basic knowledge regarding organic chemistry and work in a organic chemistry laboratory, doesn’t follow safety rules at the laboratory;

score 3 (satisfactory): student has limited knowledge regarding organic chemistry and work in a organic chemistry laboratory, follows safety rules at the laboratory;

score 4 (good): student has basic knowledge regarding organic chemistry and work in a organic chemistry laboratory, follows safety rules at the laboratory;

score 5 (very good): student has adopted and is able to use knowledge regarding organic chemistry and work in a organic chemistry laboratory, follows carefully safety rules at the laboratory;

Skills (BI_U04, BI_U06):

score 2 (not satisfactory): student is not able to perform simple chemical experiments

score 3 (satisfactory): student is able to perform simple chemical experiments on a basic level;

score 4 (good): student is able to perform simple chemical experiments;

score 5 (very good): student is able to fluently perform simple chemical experiments;

Competencies (BI_K02, BI_K06)

score 2 (not satisfactory): student does not cooperate and work with others

score 3 (satisfactory): student is able to cooperate and work with others on a basic level

score 4 (good): student cooperates and works well with others

score 5 (very good): student cooperates and works well with others, is able to play different roles in the group